WebbThis can result in a continuous release of water during the titration of such samples, which leads to incorrect and non-reproducible results. Other samples can cause side … Webb31 dec. 2024 · For oils and fuels, it is important to note that oils contain additives for performance, which not only lead to poor solubility in common alcohol-based Karl Fischer reagents, but also often cause side reactions during titration that lead to …
Water determination in aldehydes and ketones using Karl Fischer ...
WebbKarl Fischer titration is a universal method for water content determination in technical products (plastics, oil, gases), cosmetic products, pharmaceutical ... WebbExtracting all water content, maintaining a pH range between 5 and 7, and avoiding side reactions in the solvent system are critical to the accurate determin... slucare south grand
Karl Fischer Titration of Pharmaceutical Products with Pyridine …
Webb11 juni 2024 · 1 Introduction Despite its application for decades and its great practical importance the Karl Fischer (KF) titration method, that is, the reactions taking place in … Webbrl Fischer reaction . 5 A few years later Smith et al. 3. showed that methanol played an active role in the Karl Fischer reaction and that the stoichiometry between water and … WebbThis side reaction, caused by the disproportionation of iodine molecules above pH 8, can be avoided through additional buffering of the working medium with a weak acid. … soil resistivity test standard